Proses Penghilangan Surfaktan dengan Metode Ekstraksi Pelarut Pada Sintesis Silika Mesopori MCM-41
DOI:
https://doi.org/10.68115/reprokimia.v4i1.81Keywords:
Silika Mesopori, surfaktan, template, ekstraksi pelarutAbstract
Mesoporous silica has been synthesized by using sodium silicate as silica source and cetiltrimetilammonium bromide (CTAB) as a molecular template agent. Mesoporous silica synthesized at pH 11 with a molar ratio of SiO2 with CTAB was 1: 0.53 through hydrothermal method. In this study, the removal of the surfactant has been done through solvent extraction process. Characterization of the sample with X-Ray Diffraction (XRD) showed that the mesoporous silica has been synthesized by the emergence of a pattern that is typical for mesoporous material, spectra Fourier Transform Infra-Red (FTIR) still shows the presence of surfactant molecules on silica calcination. Results of Scanning Electron Microscopy (SEM) showed morphology of spherical-shaped surface with a uniform particle size distribution.
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